ONE-STEP SYNTHETIC OFP-TERT-BUTYLCALIX[4]ARENE DERIVATIVE VIA DIRECT BENZOYLATION: MECHANISM REACTION STUDIES
- Department of Chemistry, Faculty of Mathematics- and Natural Sciences, Jember UniversityJl. Kalimantan 37, Jember Indonesia 681752.
- Departement of Chemistry, Faculty of Mathematics and Natural Sciences, Gadjah Mada University.
Abstract
The aim of research the synthesis of 5,11,17,23-tetra(t-butyl)-25-monohydroxy-26,27,28-tribenzoyloxycalix[4]arene (TBMTCA) material were by one-step synthesized by benzoylation reaction of 5,11,17,23-tetra(t-butyl)-25,26,27,28-tetrahydroxycalix[4]arene (TBCA) and benzoyl chloride is (1: 3,7) mol and the refluxing 3 hours at room temperature and predicted mechanism reaction models. The product reaction of synthesis was carried out by means of FTIR and 1H-NMR spectroscopy. The results material of5,11,17,23-tetra(t-butyl)-25-monohydroxy-26,27,28-tribenzoyloxycalix[4]arene (TBMTCA)synthesized was light yellow crystalline having melting point 306-3090C in 90,2 % yields.
Keywords
Article Analytics
How to Cite This Article
Busroni, Sri Juari Santosa and Chairil Anwar (2022); ONE-STEP SYNTHETIC OFP-TERT-BUTYLCALIX[4]ARENE DERIVATIVE VIA DIRECT BENZOYLATION: MECHANISM REACTION STUDIES, Int. J. of Adv. Res., 10 (11), 207-210, ISSN 2320-5407. DOI: https://doi.org/10.21474/IJAR01/15659
Corresponding Author
This work is licensed under a Creative Commons Attribution 4.0 International License.