Vol. 5 (04) pp. 234-241 DOI: 10.21474/IJAR01/3800

A KINETIC STUDY OF RUBAZOIC ACID FORMATION DERIVED FROM 4-AMINO-1(4-SULPHOPHENYL) 3-METHYL-2-PYRAZOLIN-5-ONE.

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  • Institute of Chemistry, University of the Punjab, Lahore 54590, Pakistan.
  • Department of Chemistry, University of Management and Technology Lahore-54000, Pakistan.
  • Department of Chemistry, GC University, Kachehry Road, Lahore 54000, Pakistan.
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Abstract

A kinetic study based on spectrophotometric and titrimetric techniques has been carried out for the formation of Rubazoic acid (4E)-4-[(5-hydroxy-3-methyl-1-phenyl-4,5-dihydro-1H-pyrazol-4-yl)imino]-5-methyl-2-phenyl-2,4 dihydro-3H-pyrazol-3-one from 4-amino-1(4-sulphophenyl) 3-methyl-2-pyrazolin-5-one. Physicochemical factors like effect of time, pH, aeration and temperature on its formation have been investigated in detail. Elemental analysis, UV-Visible spectral study, FTIR spectral study, 1H-NMR and 13C-NMR spectral study was employed for understanding the reaction path way for the formation of rubazoic acid.

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How to Cite This Article

Ghulam Hussain, Shakeel Ahmad Khan, Waqar Ahmad, Makshoof Athar and Rashid Saleem. (2017); A KINETIC STUDY OF RUBAZOIC ACID FORMATION DERIVED FROM 4-AMINO-1(4-SULPHOPHENYL) 3-METHYL-2-PYRAZOLIN-5-ONE., International Journal of Advanced Research (IJAR), 5 (04), 234-241, ISSN 2320-5407. DOI: https://doi.org/10.21474/IJAR01/3800

Corresponding Author

Shakeel Ahmad Khan
Department of chemistry, University of Management and Technology Lahore-54000, Pakistan

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