COMPARISON AND EVALUATION OF FLEXURAL STRENGTH OF HEAT POLYMERIZED ACRYLIC RESIN AFTER REPAIR WITH ZIRCONIA OXIDE AND ALUMINIUM OXIDE REINFORCED AUTOPOLYMERIZING ACRYLIC RESIN WITH TWO DIFFERENT REPAIR DESIGNS AND WITH AND WITHOUT SURFACE TREATMENT - AN INVITRO STUDY

  • Postgraduate Student, Department of Prosthodontics, Co.org. Institute of Dental Sciences, Karnataka, India.
  • Professor & H.O.D, Department of Prosthodontics, Co.org. Institute of Dental Sciences, Karnataka, India.
  • Professor & Chair, Department of Prosthodontics, Co.org. Institute of Dental Sciences, Karnataka, India.
  • Reader, Department of Prosthodontics, Co.org. Institute of Dental Sciences, Karnataka, India.
  • Senior Lecturer, Department of Prosthodontics, Co.org. Institute of Dental Sciences, Karnataka, India.
  • Abstract
  • Keywords
  • References
  • Cite This Article as
  • Corresponding Author

Aim: The aim of this study was to evaluate and compare flexural strength of repaired heat polymerized acrylic resin with zirconia oxide and aluminium oxide nanoparticles incorporated autopolymerized acrylic resin and to evaluate effect of butt and bevel joint design of repair with and without chemical surface treatment. Materials and Method: A total of 165 heat cure acrylic resin specimens were fabricated and divided into 3 main groups. Group A had 15 intact specimens whereas group B and group C were further divided into 5 subgroups depending on repair material, repair design and chemical surface treatment used. Each subgroup had 15 specimens. 7wt% zirconia oxide and 2wt% aluminium oxide nanoparticles used as reinforcement material into autopolymerized acrylic resin and compared with unreinforced autopolymerized resin used for repair. Butt and bevel joint designs and ethyl acetate as a chemical surface treatment used for repair of acrylic specimens. The specimens were subjected to flexural strength in a universal testing machine until specimens fractured and load values were recorded. Flexural strength wascalculated in MPa (Megapascal) and analysed using Independent t test, One Way ANOVA and Post hoc Tukey?s test. Results: The flexural strength values obtained were highly significant for nanoparticles reinforced groups than unreinforced autopolymerized resin. Also zirconia oxide nanoparticles showed higher values than aluminium oxide nanoparticles. Similarly, repair with bevel joint design and with chemical surface treatment with ethyl acetate proved to be better. Conclusion: Under the conditions of this study, 7wt% zirconia oxide and 2wt% aluminium oxide reinforced autopolymerized resin with bevel joint design and chemical surface treatment with ethyl acetate can be recommended for acrylic repair.


  1. Gad MM, Rahoma A, Thobity AM, ArRejaie AS. Influence of incorporation of ZrO2 nanoparticles on the repair strength of polymethyl methacrylate denture base. Int J Nanomedicine. 2016 Oct; 27(11):5633-43.
  2. Arora N, Jain V, Chawla A, Mathur VP. Effect of addition of sapphire (aluminium oxide) or silver fillers on the flexural strength thermal diffusivity and water sorption of heat polymerized acrylic resins. IJOPRD. 2011 Apr-Jun; 1(1):21-7.
  3. Hamza T, Wee AG, Alapati S, Schricker SR. The fracture toughness of denture base material reinforced with different concentrations of POSS. J Macromol Sci. Part A Pure Appl Chem. 2004; A 41(8): 897-906, DOI: 10. 1081/MA-120039176.
  4. Gad M, ArRejaie AS, Abdel-Halim MS, Rahoma A. The reinforcement effect of nanozirconia on the transverse strength of repaired acrylic denture Base. Int J Dent. 2016 May; volume 2016:1-6.Article ID 7094056.doi:10.1155/2016/7094056.
  5. Sarac YS, Sarac D, Kulunk T, Kulunk S. The effect of chemical surface treatments of different denture base resins on the shear bond strength of denture repair. J Prosthet Dent. 2005 Sep; 94(3):259-66.
  6. Yadav NS, Khare S, Mishra SK, Vyas R, Mahajan H, Chitumalla R. In-vitro evaluation of transverse strength of repaired heat cured denture base resins without surface treatment and with chemical and mechanical surface treatment. J Int Oral Health. 2015 Aug; 7(8):89-92.
  7. Saritha MK, Shadakshari S, Nandeeshwar DB, Tewary S. An in vitro study to investigate the flexural strength of conventional heat polymerised denture base resin with addition of different percentage of aluminium oxide powder. Asian J Med Clin Sci. 2012 May-Aug; 1(2):80-5. 15.
  8. Pan Y, Liu F, Xu D, Jiang X, Yu H, Zhu M. Novel acrylic resin denture base with enhanced mechanical properties by the incorporation of PMMA-modified hydroxyapatite. Progress in Natural Science: Materials International. 2013 Feb;23(1):89-93.
  9. Berrong JM, Weed RM, Young JM. Fracture resistance of kevlar-reinforced poly (methyl methacrylate) resin: A preliminary study. Int J Prosthodont. 1990; 3(4): 391-5.
  10. Narva KK, Lassila LV, Vallittu PK. The static strength and modulus of fiber reinforced denture base polymer. Dent Mater. 2005 May; 21(5):421-8. 18.
  11. Franklin P, Wood DJ, Bubb NL. Reinforcement of poly (methyl methacrylate) denture base with glass flake. Dent Mater. 2005 Apr; 21(4):365-70.
  12. Ayaz EA, Durkan R. Influence of acrylamide monomer addition to the acrylic denture-base resins on mechanical and physical properties. Int J Oral Sci. 2013 Dec; 5(4):229-35.
  13. Asar NV, Albayrak H, Korkmaz T, Turkyilmaz I. Influence of various metal oxides on mechanical and physical properties of heat-cured polymethyl methacrylate denture base resins. J AdvProsthodont. 2013 Aug; 5(3):241-7.
  14. Gad MM, Fouda MM, Al-Harbi FA, N?p?nkangas R, Raustia A. PMMA denture base material enhancement: A review of fiber, filler, and nanofiller addition. Int J Nanomedicine. 2017 May; 17(12):3801-12.
  15. Wang W, Liao S, Zhu Y, Liu M, Zaho Q, Fu Y. Recent applications of nanomaterials in prosthodontics. J Nanomater 2015 Mar; volume 2015. Article ID 408643.doi:1155/2015/408643.
  16. Ellakwa AE, Morsy MA, El-Sheikh AM. Effect of aluminium oxide addition on the flexural strength and thermal diffusivity of heat-polymerized acrylic resin. J Prosthodont. 2008 Aug; 17(6):439-44.
  17. Chaijareenont P, Takahashi H, Nishiyama N, Arksornnukit M. Effect of different amounts of 3-methacryloxypropyltrimethoxysilane on the flexural properties and wear resistance of alumina reinforced PMMA. Dent Mater J. 2012 Aug; 31(4): 623-8. 23.
  18. Kamble VD, Parkhedkar RD, Mowade TK. The effect of different fiber reinforcements on flexural strength of provisional restorative resins: an in-vitro study. J AdvProsthodont. 2012 Feb; 4(1):1-6.
  19. Alkurt M, Duymus ZY, Gundogdu M. Effect of repair resin type and surface treatment on the repair strength of heat- polymerized denture base resin. J Prosthet Dent. 2014 Jan; 111(1):71-8.
  20. Bural C, Bayraktar G, Aydin I, Yusufoglu I, Uyumaz N, Hanzade M. Flexural properties of repaired heat-polymerising acrylic resin after wetting with monomer and acetone. Gerodontology 2010 Sep; 27(3):217-23.
  21. Diaz-Arnold AM, Vargas MA, Shaull KL, Laffoon JE, Qian F. Flexural and fatigue strengths of denture base resin. J Prosthet Dent. 2008 July; 100(1):47-51.
  22. Ahmed MA, Ebrahim MI. Effect of zirconium oxide nano-fillers addition on the flexural strength, fracture toughness, and hardness of heat-polymerized acrylic resin. WJNSE. 2014 June; 4(2):50-7.
  23. Acosta-Torres LS, Lopez-Marin LM, Nunez-Anita RE, Hernandez-Padron G, Castano VM. Biocompatible metal-oxide nanoparticles: nanotechnology improvement of conventional prosthetic acrylic resins. J Nanomater. 2011 Jan; Volume 2011:1-8. Article ID 941561. doi:10.1155/2011/941561.
  24. Kanie T, Arikawa H, Fuji K, Ban S. Flexural properties of denture base polymers reinforced with a glass cloth-urethane polymer composite. Dent Mater. 2004 Oct; 20(8):709-16.
  25. Pereira RP, Delfino CS, Butignon LE, Vaz MAK, Arioli-Filho JN. Influence of surface treatments on the flexural strength of denture base repair. Gerodontology 2012 Jun; 29(2):e234-38.
  26. Seo RS, Neppelenbroek KH, Filho JNA. Factors affecting the strength of denture repairs. J Prosthodont. 2007 July-Aug; 16(4):302-10.
  27. Jasim, B., S., Ismail, I. J. The Effect of Silanized Alumina Nano-Fillers Addition on Some Physical and Mechanical Properties of Heat Cured Polymethyl Methacrylate Denture Base Material. Restorative Dentistry 2014;26(2):18-23.
  28. Vallittu PK, Lassila VP, Lappalainen R. Wetting the repair surface with methyl methacrylate affects the transverse strength of repaired heat-polymerized resin. J Prosthet Dent 1994;72:639-43.
  29. Ward JE, Moon PC, Levine RA, et al: Effect of repair surface design, repair material, and processing method on the transverse strength of repaired acrylic denture resin. J Prosthet Dent 1992;67:815-820.
  30. Kanie T, Fujii K, Arikawa H, Inoue K. Flexural properties and impact strength of denture base polymer reinforced with woven glass fibers. Dent Mater. 2000 Mar; 16(2):150-8.
  31. Paleari AG, Marra J, Pero AC, Rodriguez LS, Ruvolo-Filho A, Compagnoni MA. Effect of incorporation of 2-tert-butylaminoethyl methacrylate on flexural strength of a denture base acrylic resin. J Appl Oral Sci. 2011 May-Jun; 19(3):195-9.
  32. Asopa V, Suresh S, Khandelwal M, Sharma V, Asopa SS,Kaira LS. A comparative evaluation of properties of zirconiareinforced high impact acrylic resin with thatof high impact acrylic resin. Saudi Dent J. 2015 Mar; 6:146-51.
  33. Alnamel HA, Mudhaffer M. The effect of Silicon di oxide Nano -Fillers reinforcement on some properties of heat cure polymethyl methacrylate denture base material.J BaghColl Dentistry 2014 Mar; 26(1):32-36.
  34. Cilingir A, Bilhan H, Geckili O, Sulun T, Bozdag E, Sunbuloglu E. In vitro comparison of two different materials for the repair of urethandimethacrylate denture bases. J AdvProsthodont. 2013 Nov; 5(4):396-401.
  35. Balos S,Pilic B, Markovic D, Pavlicevic J,Luzanin O. Polymethyl-methacrylatenanocomposites with low silica addition. J Prosthet Dent 2014; 111:327-34.

[Khot Kalyani Jalindar, Basavaraj S. Salagundi, Rupesh P.L, Mallikarjuna D.M, Unni Pympallil and Pallavi N.T (2020); COMPARISON AND EVALUATION OF FLEXURAL STRENGTH OF HEAT POLYMERIZED ACRYLIC RESIN AFTER REPAIR WITH ZIRCONIA OXIDE AND ALUMINIUM OXIDE REINFORCED AUTOPOLYMERIZING ACRYLIC RESIN WITH TWO DIFFERENT REPAIR DESIGNS AND WITH AND WITHOUT SURFACE TREATMENT - AN INVITRO STUDY Int. J. of Adv. Res. 8 (Feb). 973-987] (ISSN 2320-5407). www.journalijar.com


DR. KHOT KALYANI JALINDAR
POST GRADUATE

DOI:


Article DOI: 10.21474/IJAR01/10533      
DOI URL: https://dx.doi.org/10.21474/IJAR01/10533