SYNTHESIS, SPECTROSCOPIC STUDIES (FTIR AND UV-VISIBLE), CRYSTAL STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF A NEW INORGANIC-ORGANIC HYBRID MATERIAL BASED ON A B-OCTAMOLYBDATE CLUSTER (C12H28N)4[MO8O28].3H2O
- Laboratoryof Mineral and Analytical Chemistry, Department of Chemistry, Faculty of Sciences and Technology, Cheikh Anta Diop University, Dakar, Senegal.
- Laboratory of Organic Physical Chemistry and Environmental Analyses (LCPOAE), Department of Chemistry, Faculty of Sciences and Technology, Cheikh Anta Diop University, Dakar, Senegal .
- Service commund analyse par diffraction des rayons X, Universite de Bretagne occidentale, 6, avenue Victor Le Gorgeu, CS 93837, F-29238 BREST cedex 3, France.
Abstract
A new organic-inorganic hybrid material based on a B-octamolybdate cluster(C12H28N)4[Mo8O28].3H2O,has been synthesized from ammonium heptamolybdate tetrahydrate (NH4)6Mo7O24.4H2O, iodic acid HIO3 and dihexylamine[CH3 (CH2)5 NH (CH2)5CH3 at 388K,then characterized by spectroscopic studies (FTIR and UV-Visible) and confirmed by single crystal X-ray diffraction (XRD). Thus, the redox properties of the compound were also been studied by cyclic voltammetry in H2SO4 (1M) at a scanning speed of 40 mV/s using glassy carbon as a reference electrode and the results show two reversible redox peaks corresponding probably two electrons from Mo centers.
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How to Cite This Article
Mamadou Ba, Waly Diallo, Bougar Sarr, Balla Fall, Bocar Traore, Abdoul Khadir Diop Mamadou Sidibe and Francois Michaud (2025); SYNTHESIS, SPECTROSCOPIC STUDIES (FTIR AND UV-VISIBLE), CRYSTAL STRUCTURE AND ELECTROCHEMICAL PROPERTIES OF A NEW INORGANIC-ORGANIC HYBRID MATERIAL BASED ON A B-OCTAMOLYBDATE CLUSTER (C12H28N)4[MO8O28].3H2O , Int. J. of Adv. Res., 13 (08), 1484-1493, ISSN 2320-5407. DOI: https://doi.org/10.21474/IJAR01/21647
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